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Solvent casting was completed employing a casting knife applicator from Elcometer (Rochester Hills, Michigan, North The united states) on warmth-resistant borosilicate glass. Each of the methods had been carried out within a chemical laboratory where by ambient situations of eighteen° ± two °C and R.H. 20 ± 5% have been mentioned. The residual moisture content material during the films soon after drying was calculated using Karl Fischer titration.
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Even though speedy plastic deformation could cause a temperature increase, at relatively sluggish strain-premiums the linked temperature increase is negligible. A totally adiabatic Investigation revealed an upper sure temperature raise of only 3.six °C (see Supplementary Part three.3). The mechanically activated polymer mobility well down below Tg is mechanistically fairly diverse from molecular mobility at temperatures earlier mentioned Tg, and The important thing discrepancies is usually summarized as follows: Diffusion largely happens resulting from large kinetic Strength on the polymer chains (or segments), and available free of charge-quantity (or Bodily Place) resulting from which chains (or segments) can sample new orientations successfully. The polymer melts (previously mentioned Tg) are spatially homogeneous As well as in a thermodynamic equilibrium state, whereas, plastic deformation and involved Improved mobility within a glassy polymer is in no way an equilibrium concept. The root necessarily mean sq. displacement of center of mass of the polymer chain will maximize monotonically with time all through diffusion within a polymer soften, even so, the mechanically assisted enhanced mobility in polymers only takes place all through active plastic deformation and correctly ceases when plastic straining stops. The normal kinetic energy of the polymer molecule is huge inside a polymer melt compared to that from the stable-state glass properly beneath Tg.
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